Water Vapor Transmission Rate Tester – Infrared (TDLAS) Method
Wavelength-modulated tunable diode laser absorption spectroscopy (TDLAS) with a 20 m ultra-long optical path for trace water; automatic attenuation compensation means no periodic recalibration, and medium/high-barrier materials are tested fast.
Purpose | What it does for you
Determines water vapour transmission rate, permeance and permeability of films, sheets and containers made of plastic, fabric, leather or metal. As a sensor method, it does not wait tens of hours for mass accumulation as the gravimetric method does — a single specimen typically finishes within hours, suiting labs with fast R&D iteration and many samples, while keeping good accuracy on medium and high barrier materials.
Key Features
- Wavelength-modulated TDLAS infrared trace-water sensor with 20 m ultra-long optical path, high accuracy
- Automatic attenuation compensation: no periodic recalibration, no continuous data decay
- Fully automatic fog-free humidity control 35–90% RH; semiconductor bidirectional temperature control
- Strong environmental adaptability: indoor 10–30 °C, no humidity requirement, low running cost
- Pneumatic H-type sample clamping with anti-leak sealing technology
- One-key start, fully intelligent; data preserved on power loss; power-on self-check
- Graphical all-element monitoring and multi-format reports; optional GMP Computerized System module
Operating Principle
Nitrogen at a controlled humidity flows on one side of the specimen while dry nitrogen (carrier gas) flows at a fixed rate on the other. The humidity difference drives water vapour from the high-humidity side to the low-humidity side, and the permeated vapour is carried to the infrared sensor. The sensor measures vapour concentration in the carrier gas, from which WVTR and related parameters are calculated. The core is a wavelength-modulated TDLAS trace-water sensor with a 20 m absorption path and automatic attenuation compensation, so no periodic recalibration is needed.
Technical Specifications
| Measurement Range | Film 0.005–100 g/m²·24h; container 0.00005–0.5 g/pkg·24h |
|---|---|
| Measurement Resolution | Film 0.001 g/m²·24h; container 0.00001 g/pkg·24h |
| Temperature Range | 15–45 ℃ |
| Temperature Error | ±0.3 ℃ |
| Humidity Range | 0% RH,35%–90% RH / 0% RH, 35%–90% RH |
| Humidity Error | ±2% RH |
| Specimen Thickness | <3 mm |
| Operating Environment | indoor 10–30 ℃ |
| Carrier Gas | 99.999% high-purity N₂ |
| Flow Rate | carrier gas 0–100 or 0–300 cm³/min |
| Gas Supply Pressure | 0.1–0.2 MPa |
| Interface Size | 1/8 in metal tube |
| Power Supply | AC 220/110 V ±10%,50/60 Hz |
| Power | <1.5 kW |
Note: Due to continuous product iteration and varying application conditions, the technical parameters on this page are typical reference values and are not to be used as acceptance criteria. For tender and customized projects, the product model, configuration and specifications are subject to the mutually confirmed technical agreement and the actual delivered product. For parameter matching tailored to your specific project, please contact us.
Models & Configuration
| Model | W-IR-11-G | W-IR-31-H | W-IR-41-G |
|---|---|---|---|
| Specimen Count | 1 | 3 | 4 |
| Test Area | 50.0 cm² | 38.48 cm² | 50.0 cm² |
| Dimensions | 415×720×400 mm | 520×778×475 mm | 415×720×400 mm |
| Net Weight | 66 kg | 80 kg | 90 kg |
Standard Configuration
Mainframe, test computer, professional software, water trap, sampler, nitrogen cylinder regulator, sealing grease. Optional: container test kit, container temperature control kit, specimen masks (7 cm² / 1 cm²). User supplies high-purity nitrogen and distilled water.
Application Scenarios
- WVTR evaluation of high-barrier pharmaceutical laminates and metallised films
- Rapid screening and formulation iteration in new film development
- Moisture barrier assessment of electronic and photovoltaic encapsulation films
- Time-critical incoming sampling of flexible food packaging
Compliance Standards
Industries Served
- Pharmaceutical & Biopharmaceutical
- Food & Condiments
- Packaging & Printing
- Material R&D, Universities & Institutes
- Third-Party & Government Testing Institutes
- Medical Devices
- Building Materials & Construction
Frequently Asked Questions
Does the infrared method need periodic calibration, and is it complicated?
No periodic recalibration is required. The sensor performs automatic attenuation compensation, so data do not decay continuously over time. Routine work is limited to a verification with a reference film per your SOP — much less maintenance than sensors needing frequent calibration.
Do I need nitrogen, and is gas consumption costly?
Yes — 99.999% high-purity nitrogen as carrier gas at 0.1–0.2 MPa and 0–100 (or 0–300) cm³/min. One standard cylinder lasts a considerable time for a single instrument, so running cost is manageable; a central gas supply makes it even easier.
Compared with the cup method, when is the infrared method the better choice?
The infrared (TDLAS) method is a sensor method: it does not wait for mass to accumulate, so a single specimen typically finishes within hours, whereas the cup method can take days on high-barrier materials. Its ranges are 0.005–100 g/m²·24h for films and 0.00005–0.5 g/pkg·24h for containers, with resolutions of 0.001 and 0.00001 respectively. Three situations favour it: high-barrier structures (metallised film, foil laminates, oxide-coated films); R&D and incoming inspection that need fast answers; and labs with high test throughput. Where the number must go into a regulatory file and needs absolute-method backing, gravimetric remains the more defensible reference.
How do I choose between the gravimetric cup, electrolytic and infrared WVTR methods?
Choose by range and purpose. The gravimetric cup method is closest to the pharmacopoeia and ASTM E96 classic: a wide range, finished containers can be measured directly, but each run is long — best for compliance comparison and referee testing. The electrolytic method is an absolute coulometric method suited to low-transmission films and containers. The infrared (TDLAS) method responds fast and suits trace water vapour in high-barrier materials and high-throughput work. Pick the cup method when compliance leads, electrolytic or infrared when line efficiency leads.
What is the difference between differential-pressure and equal-pressure (coulometric) gas transmission testing?
The differential-pressure method creates a pressure difference across the specimen and tracks the pressure rise on the low-pressure side; one instrument measures oxygen, carbon dioxide, nitrogen and other non-toxic gases, making it the general-purpose choice. The equal-pressure method keeps both sides at the same pressure and uses a coulometric sensor for oxygen only, giving higher sensitivity for the extremely low OTR of high-barrier materials. Two rules: choose differential pressure when you need several gases, coulometric when you measure oxygen only and need the lowest detection limit.
Why does high-barrier gas transmission testing take so long?
Because the transmitted amount is extremely small, you must wait until permeation reaches steady state and the accumulated signal exceeds the instrument resolution; temperature and humidity equilibration and the system background (residual oxygen or water vapour) also take time. Practical ways to shorten it: raise the test temperature and note it in the report, reduce background and leaks, use a more sensitive sensor, and add parallel test chambers. No speed-up should compromise the steady-state criterion.
How much do temperature and humidity conditions affect barrier results?
The effect is significant: conditions must match the method standard and be stated in the report. Higher temperature raises transmission; for hydrophilic materials, a change in relative humidity markedly changes both water vapour and oxygen transmission. This instrument controls 15–45 °C to ±0.3 °C and covers 35%–90% RH (some models also offer 0% RH). Before comparing data between laboratories, check that both used the same temperature and humidity.
Does LabStone support OEM/ODM and customised instruments?
Yes. Standard models ship as-is, while chamber count, specimen size, fixtures, temperature range and software modules (including the GMP Computerized System module) can be tailored to your SOP and URS. IQ/OQ/PQ validation documentation packages are available.
What is the typical lead time, and how is shipping handled?
Standard models usually ship in 4–8 weeks; customised builds depend on the agreed scope. Instruments are packed in export wooden cases and can move by sea, air or rail. We supply proforma invoice, packing list and certificate of origin (CO / Form E), and work under EXW, FOB, CIF or DAP terms.
How are installation, training and calibration handled after delivery?
We provide remote installation guidance, bilingual (Chinese/English) manuals and video training; on-site commissioning by our engineers is available. Users can self-calibrate with standard weights, reference films or calibrated leak standards, and third-party calibration certificates can be supplied.
What is the warranty, and how are spare parts supplied?
The instrument carries a 12-month warranty from acceptance plus lifetime maintenance support. Consumables (molecular sieve, desiccant, sealing grease, printer paper) are kept in long-term stock, and key components are international brands available worldwide. We respond to technical enquiries within 24 hours.
Do the instruments comply with ASTM, ISO and pharmacopoeia standards?
Yes. Every instrument lists its applicable standards on the specification page (ASTM, ISO, GB, YBB, Chinese Pharmacopoeia, USP, EP, JIS, DIN, TAPPI and more). The software outputs raw records and reports suitable for audit trails, with an optional GMP / FDA 21 CFR Part 11 compliance module.
Which languages does the software support, and can it integrate with a LIMS?
The software ships with Chinese and English interfaces; other languages can be added on request. Data export is available over RS232, USB, Ethernet or Wi-Fi, and reports can be exported to Excel, PDF or structured files for LIMS integration.